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Home⇒ Medical Science⇒ Biochemistry⇒ Gas chromatography
1-Dont try to cram or spend more time here just read it fast and cover syllabus then practice MCQ's cheptor of same topic to check your progress. . |
2-Wrong options are also given but dont concentrate there, Right answer is in bold format. |
Q1 ⇒ Which of the following detectors give concentration-dependent signals? All of these [other wrong options] [Discuss in forum] ![]() ![]() Electron-capture detector Thermal conductivity Infra-red detector |
Q2 ⇒ Headspace analysis is carried out in order to analyse volatile compounds from solid or liquid samples [other wrong options] [Discuss in forum] ![]() ![]() determine the psychological state of the tutor analyse the column contents ahead of the sample determine non-volatiles |
Q3 ⇒ Column bleeding occurs when traces of the stationary phase are eluted [other wrong options] [Discuss in forum] ![]() ![]() elution of the analyte is extended over time the column is cracked and stationary phase leaks out the column breaks during installation and causes personal injury |
Q4 ⇒ Derivatisation of a sample is carried out to all of the above [other wrong options] [Discuss in forum] ![]() ![]() reduce polarity of the analytes increase the detector response increase volatility of the analytes |
Q5 ⇒ What does the selectivity factor describe? The relative separation achieved between two species [other wrong options] [Discuss in forum] ![]() ![]() The proportional difference in widths of two chromatographic peaks The maximum number of different species which a column can separate simultaneously None of the above |
Q6 ⇒ Which of the following gases is unsuitable for use as a GC carrier gas? Oxygen [other wrong options] [Discuss in forum] ![]() ![]() Nitrogen Helium All of the above |
Q7 ⇒ What is the typical internal diameter of fused silica capillary columns? 0.2-0.3 mm [other wrong options] [Discuss in forum] ![]() ![]() 0.3-0.5mm 0.5-1.0 mm 1.0-2.0 mm |
Q8 ⇒ What does the retention factor, k', describe? The migration rate of an analyte through a column [other wrong options] [Discuss in forum] ![]() ![]() The distribution of an analyte between the stationary and the mobile phase The velocity of the mobile phase All of these |
Q9 ⇒ Doubling the column's length increases resolution by a factor of (2)0.5 [other wrong options] [Discuss in forum] ![]() ![]() 2 3 4 |
Q10 ⇒ The GC trace obtained after an experiment is called a chromatogram [other wrong options] [Discuss in forum] ![]() ![]() chromatograph chromatophore graph |
Q11 ⇒ Which of the following detectors give mass flow-dependent signals? Field ionisation detector [other wrong options] [Discuss in forum] ![]() ![]() Electron capture detector Thermal conductivity detector All of the above |
Q12 ⇒ Sample retention in the column is measured by all of these [other wrong options] [Discuss in forum] ![]() ![]() retention time retention factor retention index |
Q13 ⇒ Which of the following is not used for detection in GC? NMR [other wrong options] [Discuss in forum] ![]() ![]() Infrared spectroscopy Flame ionisation Electrical conductivity |
Q14 ⇒ In column switching chromatography compounds trapped on one column are eluted to another column [other wrong options] [Discuss in forum] ![]() ![]() one column is removed and replaced by another the flow to the column is switched on and off repeatedly any of the above |
Q15 ⇒ The column is heated to all of these [other wrong options] [Discuss in forum] ![]() ![]() prevent analyte condensation within the column control elution of the different analytes reduce band broadening to get sharper peaks |
Q16 ⇒ Resolution is proportional to the square root of the number of theoretical plates in a column [other wrong options] [Discuss in forum] ![]() ![]() number of theoretical plates in a column square of the number of theoretical plates in a column cube root of the number of theoretical plates in a column |
Q17 ⇒ Theoretical plates are used to estimate the efficiency of a column [other wrong options] [Discuss in forum] ![]() ![]() determine the thickness of the stationary phase measure the distribution of the analyte between mobile and stationary phases None of the above |
Q18 ⇒ Sample injection is considered successful if the sample is concentrated at the start of the column [other wrong options] [Discuss in forum] ![]() ![]() all of the sample in the injector has been added to the column the sample is spread evenly along the column the sample is homogenously spread along the column |
Q19 ⇒ Which of these effects result from slow injection of a large sample volume? Decreased resolution [other wrong options] [Discuss in forum] ![]() ![]() Increased resolution Non-linear detector response Constant resolution |
Q20 ⇒ A retention gap is placed between the injector and the front of the column to retain contaminants and prevent them from reaching the column [other wrong options] [Discuss in forum] ![]() ![]() retain the sample and release it gradually to the column prevent backflush of the injected solution all of the above |
Or |